Exam 9: Nuclear Magnetic Resonance and Mass Spectrometry
Exam 1: The Basics158 Questions
Exam 2: Families of Carbon151 Questions
Exam 3: Acids and Bases149 Questions
Exam 4: Nomenclature and Conformations of Alkanes and Cycloalkanes163 Questions
Exam 5: Stereochemistry179 Questions
Exam 6: Nucleophilic Reactions91 Questions
Exam 7: Alkenes and Alkynes I220 Questions
Exam 8: Alkenes and Alkynes II163 Questions
Exam 9: Nuclear Magnetic Resonance and Mass Spectrometry158 Questions
Exam 10: Radical Reactions148 Questions
Exam 11: Alcohols and Ethers256 Questions
Exam 12: Alcohols From Carbonyl Compounds210 Questions
Exam 13: Conjugated Unsaturated Systems201 Questions
Exam 14: Aromatic Compounds186 Questions
Exam 15: Reactions of Aromatic Compounds207 Questions
Exam 16: Aldehydes and Ketones189 Questions
Exam 17: Carboxylic Acids and Their Derivatives213 Questions
Exam 18: Reactions at the Α Carbon of Carbonyl Compounds190 Questions
Exam 19: Condensation and Conjugate Addition Reactions of Carbonyl Compounds182 Questions
Exam 20: Amines207 Questions
Exam 21: Transition Metal Complexes86 Questions
Exam 22: Carbohydrates124 Questions
Exam 23: Lipids127 Questions
Exam 24: Amino Acids and Proteins135 Questions
Exam 25: Nucleic Acids and Protein Synthesis126 Questions
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What is the structure of the compound in the following 1H-NMR spectrum with the molecular formula C5H11NO,which shows a characteristic stretch in the IR around 1700 cm-1,and a characteristic peak at 202 ppm in the 13C-NMR? Relative integration is shown. 
(Multiple Choice)
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A compound C4H9Br gave the following 1H NMR spectrum: triplet, 1.0 (3H); doublet, 1.7; multiplet 1.8; multiplet, 4.1 (1H)
Which is a reasonable structure for the compound?
(Multiple Choice)
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An unknown compound,I,has the formula C3H7NO2.Elucidate the structure of I by scrutinizing its IR,1H NMR and 13C NMR spectra,shown below.

(Essay)
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Predict the splitting pattern you would observe for the proton at C3 of 2,3-dimethyl-2-phenylbutane. 
(Multiple Choice)
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In mass spectrometry,the most intense peak is assigned an intensity of 100%,and is referred to as the ___.
(Short Answer)
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An unknown compound,C,has the formula C7H7Br.Elucidate the structure of C by scrutinizing its IR,1H NMR and 13C NMR spectra,shown below.

(Essay)
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What is the structure of the compound in the following 1H-NMR spectrum with the molecular formula C6H10O2? Relative integration is shown. 
(Multiple Choice)
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An unknown compound,E,has the formula C6H12O.Elucidate the structure of E by scrutinizing its IR,1H NMR and 13C NMR spectra,shown below.

(Essay)
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What is the structure of the compound in the following 1H-NMR spectrum with the molecular formula C10H12O2? Relative integration is shown. 
(Multiple Choice)
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Which proton(s)of the compound below would appear as a septet in the 1H NMR spectrum? 
(Multiple Choice)
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A compound with the molecular formula C4H10O gives a 1H NMR spectrum consisting only of a quartet centered at 3.5 and a triplet at 1.1.The most likely structure for the compound is:
(Multiple Choice)
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What can be determined from the relative abundance of the M+ +1 peak?
(Essay)
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What is the structure of the compound in the following 1H-NMR spectrum with the molecular formula C9H12O? Relative integration is shown. 
(Multiple Choice)
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Interpret the following 13C/DEPT spectrum of a compound C5H10Br2: elucidate the structure and assign all the 13C resonances. 
(Essay)
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Which one of the following best represents the predicted approximate chemical shift and coupling for the hydrogen(s)indicated with the arrow in the compound nicotine? 
(Multiple Choice)
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What compound is used as the standard "zero" reference in both carbon and proton NMR?
(Essay)
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Which one of the following best represents the predicted approximate chemical shift and coupling for the hydrogen(s)indicated with the arrow? 
(Multiple Choice)
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A downfield ( 9-10)singlet is observed in the 1H NMR spectrum of:
(Multiple Choice)
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Determine the most likely structure of a compound,with the molecular formula C9H12,which gave a 1H NMR spectrum consisting of: a doublet at 1.25
A septet at 2.90 and
A multiplet at 7.25
]
(Multiple Choice)
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